N-Benzyl-N-ethylaniline

1 He wai ʻaila melemele māmā, hiki ke hoʻoheheʻe ʻia i loko o ka ethanol a me nā mea hoʻoheheʻe organik ʻē aʻe, hiki ʻole ke hoʻoheheʻe ʻia i ka wai.

2, Loaʻa ke ʻano hana ma o ka hoʻohui ʻana i ka ethyl aniline a me ka benzyl chloride. I loko o ka ipu hao i uhi ʻia me ke kēpau, e hoʻohui i ka ethyl aniline, e hoʻohui i ka benzyl chloride i ka wā e hoʻomaʻalili ai, e hoʻoulu no 10 mau hola, a laila e hoʻomehana i ka 100°C no 12 mau hola. Ma hope o ka holoi ʻana me ka hopena sodium hydroxide, loaʻa ka huahana i hoʻopau ʻia ma o ka distillation vacuum. Hiki ke hoʻohana ʻia ʻo Diethylaniline ma ke ʻano he mea maka. ʻO ka lakio molar o diethylaniline i benzyl chloride he 2:1. E hoʻohui i ka 1% o ka nui o ka diethylaniline e hoʻoulu ai me ka iodine, e hoʻohui ma 150℃ no 20h, a e distill vacuum e loaʻa ai ka huahana i hoʻopau ʻia.

3, Hoʻohana ʻia ma ke ʻano he mea hoʻoluʻu waena. Hoʻohana ʻia e hana i ka ʻōmaʻomaʻo māmā SF waikawa a me nā mea hoʻoluʻu polū ʻē aʻe.

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