N-Benzyl-N-ethylaniline

1 He wai ʻaila melemele māmā, hiki ke hoʻoheheʻe ʻia i ka ethanol a me nā mea hoʻoheheʻe ʻē aʻe, ʻaʻole hiki ke hoʻoheheʻe ʻia i ka wai.

2, Loaʻa ke ʻano hana ma ka reacting ethyl aniline a me benzyl chloride. I loko o ka ipu hao, e hoʻohui i ka ethyl aniline, e hoʻohui i ka benzyl chloride i ka wā e hoʻoluʻu ai, e hoʻonāuki no 10 mau hola, a laila e hoʻomehana i 100 ° C no 12 mau hola. Ma hope o ka holoi ʻana me ka solution sodium hydroxide, loaʻa ka huahana i hoʻopau ʻia e ka distillation vacuum. Hiki ke hoʻohana ʻia ʻo Diethylaniline ma ke ʻano he mea maka. ʻO ka ratio molar o diethylaniline me benzyl chloride he 2:1. E hoʻohui i 1% o ka nui o ka meaʻai o ka diethylaniline e hoʻopili iā ia me ka iodine, e hoʻololi i ka 150 ℃ no 20h, a e hoʻomaʻemaʻe i ka momi no ka loaʻa ʻana o ka huahana i pau.

3, Hoʻohana ʻia e like me ke kala waena. Hoʻohana ʻia no ka hana ʻana i ka ʻōmaʻomaʻo māmā SF a me nā mea pena uliuli ʻē aʻe.

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